Ethylenediamine → HCID 178511377, compound

HRID 235797Notes

Reaction equation

HRID 235797 reaction equation
[CH2:1]([NH2:4])[CH2:2][NH2:3].[CH:5]1[CH:6]=[CH:7][C:8]([C:11]2([C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=3)[NH:16][C:15]([O-:17])=[N:14][C:12]2=[O:13])=[CH:9][CH:10]=1.[Na+:24]>O>[CH:21]1[CH:20]=[CH:19][C:18]([C:11]2([C:8]3[CH:7]=[CH:6][CH:5]=[CH:10][CH:9]=3)[NH:16][C:15]([O-:17])=[N:14][C:12]2=[O:13])=[CH:23][CH:22]=1.[Na+:24].[CH2:1]([NH2:4])[CH2:2][NH2:3]

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 178518528HCID 178518528, compound

Product 1

HCID 178511377HCID 178511377, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Ethylenediamine (0.58 g, 10 mmol) was dissolved in 20 ml water, added to 1.25 g phenytoin sodium, and sonicated to dissolve the solid. When this clear solution was diluted to 25 ml, it had a pH of 11.6.

Workup

  1. customsonicated
  2. dissolutionto dissolve the solid
  3. additionWhen this clear solution was diluted to 25 ml, it

Sources & evidence

ORD record
ord-5a19ed8cbf1945098f0dd254efce3ac3
Source dataset
uspto-grants-1987_02
Patent number
US04642316

Reaction notes

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