HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butyn-1-ol → HCID 67533140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butyn-1-ol | HCID 12991 | — |
| Reactant | HCID 11536115 | HCID 11536115 | — |
| Reactant | Potassium tertbutoxide | HCID 50987170 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 67533140 | HCID 67533140 | — |
Reaction Steps
Preparation according to Example 5: 1-[3-(1-ethylpiperidin-4-yl)-2-fluorophenyl]ethanone (12 mg, 0.048 mmol), dimethylsulfoxide (1 ml), 2-butyn-1-ol (6.7 mg, 0.096 mmol), potassium-tertbutoxide (11 mg, 0.096 mmol). MS m/z (relative intensity, 70 eV) 247 (M+, 57), 232 (bp), 218 (28), 147 (24) 84 (67).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-374343d62ec147ee80e40c7a77f669b8 |
| Source note | uspto-grants-2010_07 |