HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86085872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,1,1-Trifluoro-3-iodopropane | HCID 156165 | — |
| Reactant | HCID 57448052 | HCID 57448052 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86085872 | HCID 86085872 | — |
Reaction Steps
Preparation according to Example 1: 2-piperidin-4-yl-6-(trifluoromethyl)phenol (0.01 g, 0.04 mmol), acetonitrile (2 ml), potassium carbonate (0.01 g) and 1,1,1-trifluoro-3-iodopropane (0.01 ml). MS m/z (relative intensity, 70 eV) 341 (M+, 40), 258 (bp), 195 (25), 167 (28), 152 (56).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-73ec80be2f7c4d319b6e8e4e8459855e |
| Source note | uspto-grants-2010_07 |