HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 57438797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 46315507 | HCID 46315507 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57438797 | HCID 57438797 | — |
Reaction Steps
Preparation according to preparation 6: 2-fluoro-3-pyridin-4-ylbenzamide (0.94 g, 4.34 mmol), 1-iodoethane (3 ml), ethanol (40 ml), sodium borohydride (1.25 g, 34.8 mmol). Yield: 0.75 g. MS m/z (rel. intensity, 70 eV) 248 (M+, bp), 247 (37), 233 (99), 146 (22), 110 (41).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-31d2babfcc064c82bd3a2917d3d5b7a1 |
| Source note | uspto-grants-2010_07 |