HCID 58000837, compound → HCID 178515781, compound

HRID 2358261Notes

Reaction equation

HRID 2358261 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[C:10]([C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=3[Cl:27])[N:11](O)[C:12]=2[C:13]2[CH:18]=[CH:17][NH:16][C:15](=[O:19])[CH:14]=2)=[CH:4][CH:3]=1>CO>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[C:10]([C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=3[Cl:27])[NH:11][C:12]=2[C:13]2[CH:18]=[CH:17][NH:16][C:15](=[O:19])[CH:14]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 58000837HCID 58000837, compound

Product 1

HCID 178515781HCID 178515781, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using the general procedure in Example 1 Step D, the intermediate of Example 3 Step A was treated with TiCl3 in methanol. 1H NMR (400 MHz, DMSO-d6): [M+1]+ 427.

Sources & evidence

ORD record
ord-21aae8f2321546fdbfcd6664ff4b7deb
Source dataset
uspto-grants-2010_07
Patent number
US07763634B2

Reaction notes

Loading…