HCID 58000843, compound → HCID 178515784, compound

HRID 2358267Notes

Reaction equation

HRID 2358267 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[C:10]([C:21]3[C:26]([F:27])=[CH:25][CH:24]=[CH:23][C:22]=3[F:28])[N:11](O)[C:12]=2[C:13]2[CH:18]=[CH:17][NH:16][C:15](=[O:19])[CH:14]=2)=[CH:4][CH:3]=1>CO>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[C:10]([C:21]3[C:22]([F:28])=[CH:23][CH:24]=[CH:25][C:26]=3[F:27])[NH:11][C:12]=2[C:13]2[CH:18]=[CH:17][NH:16][C:15](=[O:19])[CH:14]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 58000843HCID 58000843, compound

Product 1

HCID 178515784HCID 178515784, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using the general procedure in Example 1 Step D, the intermediate of Example 9 Step A was treated with TiCl3 in methanol to provide the title compound: [M+1]+ 428.

Sources & evidence

ORD record
ord-21286871308e486c88242b11da992bb0
Source dataset
uspto-grants-2010_07
Patent number
US07763634B2

Reaction notes

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