HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 5260199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 3-(Diphenylphosphino)-1-propylamine | HCID 280677 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 5260199 | HCID 5260199 | 98% |
Reaction Steps
Under argon, a solution of 3-diphenylphosphino-propylamine (631.2 mg, 2.6 mmol) and benzaldehyde (278.1 mg, 2.6 mmol) in ethanol (15 mL) was heated at 65° C. (oil bath) for 4 h. Then, the solvent was removed in-vacuo to give the desired product (>98% by 1H-NMR) as a white solid (822.3 mg, 2.5 mmmol, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763758B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-b53b737a75334bd4b3a4e34b23bdbdf8 |
| Source note | uspto-grants-2010_07 |