Water → Ammonium, trimethylbutyl-, hydroxide

HRID 2358507Notes

Reaction equation

HRID 2358507 reaction equation
[I-].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7].[OH2:10]>[Ag-]=O>[OH-:10].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 962WaterHCID 24398N,N,N-Trimethylbutan-1-aminium iodide

Product 1

HCID 45658Ammonium, trimethylbutyl-, hydroxide

Reagents, catalysts & solvents 1

HCID 178418778HCID 178418778, compoundCatalyst

Procedure

A typical TMBAOH solution was prepared as follows. Trimethylbutylammonium iodide, 1466.3 g, was dissolved in 1948.6 g deionized water in a 5 liter 3-necked round bottom flask equipped with overhead stirring. A 1 wt. % excess of silver(I) oxide, (99%), 712 g, was added and stirred in the dark for 24 hours. The resulting trimethylbutylammonium hydroxide solution was isolated by filtration.

Workup

  1. customA typical TMBAOH solution was prepared
  2. customequipped with overhead stirring

Sources & evidence

ORD record
ord-23715dcbdede4dc590d48a73f736771d
Source dataset
uspto-grants-2010_07
Patent number
US07763764B2

Reaction notes

Loading…