HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 5-Chloro-2-phenoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 4-Chloro-2-nitro-1-phenoxybenzene | HCID 891181 | — |
| Product | 5-Chloro-2-phenoxyaniline | HCID 66738 | 79% |
Reaction Steps
The product from Example 42a (13 g, 52.1 mmol) was reacted with SnCl2 (49.3 g, 260 mmol) following the procedure from Example 1f giving the title compound as a white solid 9.0 g, 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763731B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-c91bbec391de481ab71ec6e811e0b9e3 |
| Source note | uspto-grants-2010_07 |