HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Thiocresol → HCID 68459002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Thiocresol | HCID 7930 | — |
| Reactant | 4-Methyl-2-nitrophenyl trifluoromethanesulfonate | HCID 71346889 | — |
| Product | HCID 68459002 | HCID 68459002 | — |
Reaction Steps
The product from Example 4a (9.46 g, 33.17 mmol) was reacted with 3-methylthiophenol (4.12 g, 33.17 mmol) in place of thiophenol following the procedure from Example 1e for 18 h giving the crude title compound which was purified by silica gel column chromatography eluting with 5% EtOAc hexane providing a solid (7.50 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763731B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-2ff5b8489dc3426f83ae84635871ed8c |
| Source note | uspto-grants-2010_07 |