Benzoic acid, 3-mercapto- → HCID 64167018, compound

HRID 2358638Notes

Reaction equation

HRID 2358638 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:17]=[CH:16][C:12](C(O)=O)=[CH:11][CH:10]=2)=[C:4]([N+:18]([O-:20])=[O:19])[CH:3]=1.SC1C=C(C=CC=1)[C:25]([OH:27])=[O:26]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([CH:12]=[CH:16][CH:17]=2)[C:25]([OH:27])=[O:26])=[C:4]([N+:18]([O-:20])=[O:19])[CH:3]=1

Participants

3

Reactant 2

HCID 95737Benzoic acid, 3-mercapto-HCID 43349322HCID 43349322, compound

Product 1

HCID 64167018HCID 64167018, compoundYield 80.9%

Procedure

The product from Example 84a (0.94 g, 3.29 mmol) was reacted with 3-mercapto-benzoic acid (0.51 g, 3.31 mmol) as described in Example 84b to give the title compound (0.77 g, 80%).

Sources & evidence

ORD record
ord-95259f839cb1441baa92b7ee10da9ee9
Source dataset
uspto-grants-2010_07
Patent number
US07763731B2

Reaction notes

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