Ammonia → HCID 68458257, compound

HRID 2358639Notes

Reaction equation

HRID 2358639 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([CH:15]=[CH:16][CH:17]=2)[C:12](O)=[O:13])=[C:4]([N+:18]([O-:20])=[O:19])[CH:3]=1.[NH3:21].[CH3:22]O>>[CH3:22][NH:21][C:12](=[O:13])[C:11]1[CH:15]=[CH:16][CH:17]=[C:9]([S:8][C:5]2[CH:6]=[CH:7][C:2]([CH3:1])=[CH:3][C:4]=2[N+:18]([O-:20])=[O:19])[CH:10]=1

Participants

4

Reactant 3

HCID 222AmmoniaHCID 887MethanolHCID 64167018HCID 64167018, compound

Product 1

HCID 68458257HCID 68458257, compoundYield 96%

Procedure

The product from Example 86a (0.25 g, 0.86 mmol) was reacted as described in Example 84c substituting N-methyl amine in methanol for ammonia to give the title compound (0.25 g, 96%).

Sources & evidence

ORD record
ord-4a3d1256e5be4ee596b7c34ff70861ef
Source dataset
uspto-grants-2010_07
Patent number
US07763731B2

Reaction notes

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