HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 4-(2-amino-4-chlorophenoxy)-N,N-diethylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 4-(4-chloro-2-nitrophenoxy)-N,N-diethylbenzamide | HCID 51149700 | — |
| Product | 4-(2-amino-4-chlorophenoxy)-N,N-diethylbenzamide | HCID 68460678 | 85% |
Reaction Steps
The product from Example 129a (1.0 g, 2.87 mmol) was reduced with SnCl2 following the procedure from Example 1f giving the title compound as a clear oil (772 mg, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763731B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-1b2f390fbe33408590597163bb888ca6 |
| Source note | uspto-grants-2010_07 |