Stannous Chloride → HCID 66664995, compound

HRID 2358735Notes

Reaction equation

HRID 2358735 reaction equation
[Cl:1][C:2]1[CH:15]=[CH:14][C:5]([O:6][C:7]2[CH:12]=[CH:11][C:10]([OH:13])=[CH:9][CH:8]=2)=[C:4]([N+:16]([O-])=O)[CH:3]=1.Cl[Sn]Cl>>[NH2:16][C:4]1[CH:3]=[C:2]([Cl:1])[CH:15]=[CH:14][C:5]=1[O:6][C:7]1[CH:8]=[CH:9][C:10]([OH:13])=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 24479Stannous ChlorideHCID 129406294-(4-Chloro-2-nitrophenoxy)phenol

Product 1

HCID 66664995HCID 66664995, compoundYield 80.3%

Procedure

The product from Example 165b (1.0 g, 3.7 mmol) was reacted with SnCl2 as described in Example 1f to give the title compound (0.7 g, 78%).

Sources & evidence

ORD record
ord-b2e87a0d8194453f9cdee296d4853072
Source dataset
uspto-grants-2010_07
Patent number
US07763731B2

Reaction notes

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