HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanol → HCID 13773148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chloro-1-methylpyridinium iodide | HCID 167069 | — |
| Reactant | HCID 13392284 | HCID 13392284 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13773148 | HCID 13773148 | 77.4% |
Reaction Steps
2.0 g of 2-[2-(4-chlorophenyl)-5-(2-furyl)-4-oxazolyl]acetic acid, 2.02 g of 2-chloro-1-methylpyridinium iodide, 1.47 g of laurylalcohol, 1.60 g of triethylamine and 60 ml of tetrahydrofuran are treated in the same manner as described in Example 27. 2.4 g of lauryl 2-[2-(4-chlorophenyl)-5-(2-furyl)-4-oxazolyl]acetate are obtained. Yield: 77.4%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-4716f022c44b4bc49d48c338ed1f34ea |
| Source note | uspto-grants-1987_02 |