HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → 4-Chloro-N-[2-(furan-3-yl)-2-oxoethyl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(furan-3-yl)ethan-1-one--hydrogen chloride (1/1) | HCID 13773121 | — |
| Product | 4-Chloro-N-[2-(furan-3-yl)-2-oxoethyl]benzamide | HCID 13773122 | 100.5% |
Reaction Steps
5 g of (3-furylcarbonyl)methylamine hydrochloride, 6.0 g of sodium bicarbonate and 6.0 g of 4-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(1). 8.2 g of N-(4-chlorobenzoyl)-(3-furylcarbonyl)methylamine are thereby obtained. Yield: 100%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-5844296efd8e4889a254e1556a350f76 |
| Source note | uspto-grants-1987_02 |