HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 13773134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | N-[2-(Furan-2-yl)-2-oxoethyl]-4-methylbenzamide | HCID 13773124 | — |
| Product | HCID 13773134 | HCID 13773134 | 85.6% |
Reaction Steps
12.0 g of N-(4-methylbenzoyl)-(2-furylcarbonyl)methylamine, 2.3 g of 61% sodium hydride and 9.1 g of ethyl bromoacetate are treated in the same manner as described in Preparation 1-(2). 13.9 g of ethyl 3-(4-methylbenzoylamino)-3-(2-furylcarbonyl)propionate are thereby obtained. Yield: 85.5%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-5f3efcb50dbe4c4b93fcb9c74440d1b6 |
| Source note | uspto-grants-1987_02 |