HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 20067056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20067056 | HCID 20067056 | — |
Reaction Steps
80.8 parts of isatoic anhydride are introduced into 125 parts of dimethylacetamide, and a solution of 134.7 parts of stearylamine in 50 parts of dimethylformamide is added dropwise. When the evolution of CO2 has ended (3 hours) the resulting clear solution is stirred into 2 liters of H2O and the resulting precipitate is recrystallised from ethanol, using active charcoal. Anthranilic acid stearylamide of melting point 89°-90° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642322 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-9c8142fe5b77408a95c394638adc8152 |
| Source note | uspto-grants-1987_02 |