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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2359223Erstellt: 27. Oktober 2026

2-(3-Chloro-4,5-dimethoxyphenyl)furan → 1-(5-(3-Chloro-4,5-dimethoxyphenyl)furan-2-yl)-2-methoxy-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)ethanone

https://huagongshe.com/reaction/2359223

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-(3-Chloro-4,5-dimethoxyphenyl)furanHCID 58432001—
EduktN,2-dimethoxy-N-methyl-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)acetamideHCID 58432086—
Produkt1-(5-(3-Chloro-4,5-dimethoxyphenyl)furan-2-yl)-2-methoxy-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)ethanoneHCID 58432162—

Reaktionsschritte

1-(5-(3-Chloro-4,5-dimethoxyphenyl)furan-2-yl)-2-methoxy-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)ethanone was prepared from 2-(3-chloro-4,5-dimethoxyphenyl)furan and N,2-dimethoxy-N-methyl-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (70% EtOAc/hexanes) gave the product as a pale yellow solid (0.051 g, 12% yield). MS: m/z 469.2 [M+H]+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08685975B2
Quelldatensatzuspto-grants-2014_04
ORD IDord-e145a7a16e4d46d3a2e1adf41693a406
Quellennotizuspto-grants-2014_04