HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Bromo-3,5-dimethoxyphenyl)-5-methyloxazole → HCID 58432124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Bromo-3,5-dimethoxyphenyl)-5-methyloxazole | HCID 58431985 | — |
| Reactant | N,2-dimethoxy-N-methyl-2-(4-morpholinophenyl)acetamide | HCID 58431993 | — |
| Product | HCID 58432124 | HCID 58432124 | — |
Reaction Steps
1-(4-(4-Bromo-3,5-dimethoxyphenyl)-5-methyloxazol-2-yl)-2-methoxy-2-(4-morpholinophenyl)ethanone was prepared from 4-(4-bromo-3,5-dimethoxyphenyl)-5-methyloxazole and N,2-dimethoxy-N-methyl-2-(4-morpholinophenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (40% EtOAc-hexanes) gave the product as a yellow solid (0.048 g, 13% yield). MS: m/z 531.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685975B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-4c187cece51644d1b87cd9e2bfe08f91 |
| Source note | uspto-grants-2014_04 |