HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydro-3-furanmethanol → HCID 58495768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydro-3-furanmethanol | HCID 139980 | — |
| Reactant | HCID 58495736 | HCID 58495736 | — |
| Product | HCID 58495768 | HCID 58495768 | 67% |
Reaction Steps
Using benzyl 4-(2-{[(4-methylphenyl)sulfony]oxy}ethoxy)piperidine-1-carboxylate (4.00 g, 9.23 mmol) produced in Reference Example 1 (1c) and (tetrahydrofuran-3-yl)methanol (1.23 g, 12.0 mmol), the desired title compound (1.41 g, yield 67%) was obtained by the same method as in Examples 1 (1d) and 1 (1e).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685981B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-beda535952a2456cb70a302750251fca |
| Source note | uspto-grants-2014_04 |