Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → 4-methoxy-3-methylbenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 4-Methoxy-3-methylbenzaldoxime | HCID 4237592 | — |
| 용매 | Acetic Anhydride | HCID 7918 | — |
| 생성물 | 4-methoxy-3-methylbenzonitrile | HCID 13621613 | — |
반응 단계
A solution of 20 (30.9 g, 0.187 mole) in of acetic anhydride (200 ml) heated at reflux for 1.5 hours, cooled to room temperature and poured with vigorous stirring into 2N aqueous Na2CO3 (2 L). Overnight refrigeration gave a solid which was collected, washed with water, and dried to give 25.6 grams (93%) of 21 m.p. 48°-50°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04642311 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-1f39a2408f034349a2819aa25e755bed |
| 출처 메모 | uspto-grants-1987_02 |