HCID 13907950, compound → HCID 68555041, compound

HRID 2359858Notes

Reaction equation

HRID 2359858 reaction equation
[NH2:1][C:2]1[CH:9]=[C:8]([N:10]([CH3:12])[CH3:11])[CH:7]=[CH:6][C:3]=1[CH:4]=O.[CH3:13][O:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[CH2:21][CH2:22][C:23]#[N:24]>>[CH3:13][O:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[CH2:21][C:22]1[C:23]([NH2:24])=[N:1][C:2]2[C:3]([CH:4]=1)=[CH:6][CH:7]=[C:8]([N:10]([CH3:12])[CH3:11])[CH:9]=2

Participants

3

Reactant 2

HCID 13907950HCID 13907950, compoundHCID 18349590HCID 18349590, compound

Product 1

HCID 68555041HCID 68555041, compound

Procedure

The title compound was synthesized according to EXAMPLE 11 from 2-amino-4-dimethylaminobenzaldehyde and 3-(2-methoxyphenyl)propionitrile. The reaction was performed thermally (45 min, 70-80° C.).

Workup

  1. custom(45 min, 70-80° C.)

Sources & evidence

ORD record
ord-1563deddaff04c59b1223d86b945ac11
Source dataset
uspto-grants-2014_04
Patent number
US08686002B2

Reaction notes

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