(Dimethyl sulfide)trihydroboron → HCID 68550177, compound

HRID 2359899Notes

Reaction equation

HRID 2359899 reaction equation
[NH2:1][C:2]1[CH:19]=[C:18]([N+:20]([O-:22])=[O:21])[CH:17]=[CH:16][C:3]=1[C:4]([NH:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[O:14][CH3:15])=O.CSC.B>>[CH3:15][O:14][C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=1[CH2:7][NH:6][CH2:4][C:3]1[CH:16]=[CH:17][C:18]([N+:20]([O-:22])=[O:21])=[CH:19][C:2]=1[NH2:1]

Participants

3

Reactant 2

HCID 12423031(Dimethyl sulfide)trihydroboronHCID 68550184HCID 68550184, compound

Product 1

HCID 68550177HCID 68550177, compound

Procedure

The title compound was synthesized according to EXAMPLE 63, section 1.6 starting from 2-amino-N-(2-methoxybenzyl)-4-nitrobenzamide and borane-dimethyl sulfide.

Sources & evidence

ORD record
ord-0b5b329983fb487d86afb7fa6a4affb9
Source dataset
uspto-grants-2014_04
Patent number
US08686002B2

Reaction notes

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