Cyanogen Bromide → HCID 68553321, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:21]=[CH:20][CH:19]=[CH:18][C:4]=1[CH2:5][NH:6][CH2:7][C:8]1[CH:13]=[CH:12][C:11]([N+:14]([O-:16])=[O:15])=[CH:10][C:9]=1[NH2:17].[N:22]#[C:23]Br>>[CH3:1][O:2][C:3]1[CH:21]=[CH:20][CH:19]=[CH:18][C:4]=1[CH2:5][N:6]1[CH2:7][C:8]2[C:9](=[CH:10][C:11]([N+:14]([O-:16])=[O:15])=[CH:12][CH:13]=2)[N:17]=[C:23]1[NH2:22]Participants
3
Procedure
The title compound was synthesized according to EXAMPLE 63, section 1.8 starting from 2-[(2-methoxybenzylamino)methyl]-5-nitrophenylamine by reaction with cyanogen bromide.
Sources & evidence
- ORD record
- ord-2e74b22809ed433582b634e982c39ab6
- Source dataset
- uspto-grants-2014_04
- Patent number
- US08686002B2
Reaction notes
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