HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86652125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 25234654 | HCID 25234654 | — |
| Product | HCID 86652125 | HCID 86652125 | — |
Reaction Steps
A solution of the product from Example 125 (257 mg, 0.50 mmol) in thionyl chloride (1.5 ml) was heated at 85° C. for 40 min and then concentrated and dried in vacuo to give the title compound as a solid (0.27 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685991B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-ee31160671494391b4c25a1d01897cb9 |
| Source note | uspto-grants-2014_04 |