L-Tartaric acid → HCID 86658827, compound

Participants

Reaction Steps

Sunitinib (1.35 g, 3.39 mmol) was dissolved in boiling ethanol (140 ml), to which a solution of L-tartaric acid (0.25 g in 10 ml ethanol) was added and left to cool to room temperature to give 1.78 g of sunitinib L-tartarate. Melting point: 233-235° C. (form IV), ratio sunitinib/tartaric acid (according to NMR) 2:1.

Provenance & Evidence