HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Isocyanato-2,3-dihydro-1,4-benzodioxine → 1-Benzylindolin-5-yl 2,3-dihydro-1,4-benzodioxin-6-ylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Isocyanato-2,3-dihydro-1,4-benzodioxine | HCID 2776172 | — |
| Reactant | 1-Benzylindolin-5-ol | HCID 86659857 | — |
| Product | 1-Benzylindolin-5-yl 2,3-dihydro-1,4-benzodioxin-6-ylcarbamate | HCID 46866142 | — |
Reaction Steps
The title compound was synthesized from 1-benzylindolin-5-ol (30.0 mg, 0.133 mmol) using the same procedure employed for Example 2 (2), but with 2,3-dihydro-1,4-benzodioxin-6-ylisocyanate instead of 4-isopropylphenylisocyanate. The product was obtained as a solid (29.1 mg, 50%) having the following characteristics.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686024B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-d2b1a1776e7743959d6156d943a9e34d |
| Source note | uspto-grants-2014_04 |