Ethyl 1-bromocyclobutanecarboxylate → HCID 178424355, compound

HRID 2360209Notes

Reaction equation

HRID 2360209 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]([NH2:11])=[S:10].Br[C:13]1([C:17](OCC)=[O:18])[CH2:16][CH2:15][CH2:14]1>>[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]1[S:10][C:13]2([C:17](=[O:18])[N:11]=1)[CH2:16][CH2:15][CH2:14]2

Participants

3

Reactant 2

HCID 97595Ethyl 1-bromocyclobutanecarboxylateHCID 2787703N-(2-Methylphenyl)thiourea

Product 1

HCID 178424355HCID 178424355, compound

Procedure

Synthesis was performed from N-(2-methylphenyl)thiourea and ethyl 1-bromocyclobutanecarboxylate according to Method D.

Workup

  1. customSynthesis

Sources & evidence

ORD record
ord-889b31af7dee4b7a855652de5ce7df9f
Source dataset
uspto-grants-2014_04
Patent number
US08686011B2

Reaction notes

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