p-Octylbenzoic acid → HCID 67197771, compound

Participants

Reaction Steps

General procedure F was used to couple 0.31 mmols of H-D-Ala-OMe.HCl to 0.31 mmols of 2. The product was isolated by flash chromatography to yield 0.075 g (0.23 mmols). 1H NMR (300 MHz, CDCl3) δ 7.75 (d, J=8.1, 2H), 7.27 (d, J=8.1, 2H), 6.77 (s, 1H), 4.84 (s, 1H), 3.82 (s, 3H), 2.79-2.60 (m, 2H), 1.64 (s, 2H), 1.55 (d, J=7.1, 3H), 1.29 (s, 14H), 0.90 (t, J=6.9, 3H).

Provenance & Evidence