Decanoic Acid → HCID 86653231, compound

Participants

Reaction Steps

General procedure D was used to deprotect 0.160 g (0.94 mmols) of 4. The product was immediately carried on using general procedure F and coupled to decanoic acid (0.94 mmol, 0.162 g). The product was purified via flash chromatography to yield 0.115 g (0.51 mmols) of the title product. 1H NMR (300 MHz, CDCl3) δ 6.07 (s, 1H), 4.94 (dq, J=7.2, 14.5, 1H), 2.26-2.16 (m, 2H), 1.69-1.58 (m, 2H), 1.54 (d, J=7.2, 3H), 1.26 (d, J=6.4, 12H), 0.86 (t, J=6.7, 3H).

Provenance & Evidence