HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Chloropicolinic acid → N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-6-chloropicoline amide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Chloropicolinic acid | HCID 20812 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 6-chloropyridine-2-carbonyl Chloride | HCID 10942976 | — |
| Edukt | 2-Bromo-4-(1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl)-6-(trifluoromethyl)benzenamine | HCID 58297558 | — |
| Produkt | N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-6-chloropicoline amide | HCID 86654246 | — |
Reaktionsschritte
According to the method of 1-3 of Example 1, a target compound was prepared from 2-chloropyridine-6-carboxylic acid chloride prepared from 2-chloropyridine-6-carboxylic acid and thionyl chloride, and 2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)aniline obtained in 1-2 of Example 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08686044B2 |
| Quelldatensatz | uspto-grants-2014_04 |
| ORD ID | ord-8fe603e22d984f3389519d72c74d1d92 |
| Quellennotiz | uspto-grants-2014_04 |