HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → (Z)-1-chloro-2-undecene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 75039-83-7 | HCID 12642425 | — |
| Product | (Z)-1-chloro-2-undecene | HCID 12400864 | — |
Reaction Steps
By the procedure of example 12, (Z)-2-undecen-1-ol (13 g), 27.8 g of triphenylphosphine in 100 ml of dry CCl4 were reacted under reflux for 6.5 h. Workup as described before as in example 12 gave 12.3 g of (Z)-1-chloro-2-undecene as a colorless oil: bp 65°-66° C./0.2 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642364 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-1172915f0f4b4eea8cefa01da69b9d9d |
| Source note | uspto-grants-1987_02 |