HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-fluoroaniline → 1035689-60-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-fluoroaniline | HCID 123050 | — |
| Reactant | 3-Ethoxybenzeneboronic acid | HCID 2773920 | — |
| Product | 1035689-60-1 | HCID 66997355 | 44.2% |
Reaction Steps
The title compound (1.34 g) was prepared from 2-fluoro-4-bromo aniline (2.5 g, 13.1 mmol) and 3-ethoxyphenylboronic acid (2.8 g, 17.0 T mmol) as a pale-yellow liquid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.38-7.20 (m, 3H), 7.10 (d, J 7.9, 1H), 7.07-7.05 (m, 1H), 6.83-6.76 (m, 2H), 5.24 (s, 2H), 4.06 (q, J 7, 2H), 1.32 (t, J 7, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-a90d5f0389cf48729379cb38c3798fa5 |
| Source note | uspto-grants-2014_04 |