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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2360409Generated: October 30, 2026

4-Bromo-2,6-dichloroaniline → HCID 66996749, compound

https://huagongshe.com/reaction/2360409

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Bromo-2,6-dichloroanilineHCID 69680—
Reactant(3-Methoxyphenyl)boronic acidHCID 2734370—
ProductHCID 66996749HCID 66996749102.6%

Reaction Steps

The title compound (0.550 g) was prepared from 2,6-dichloro-4-bromoaniline (0.5 g, 2.0 mmol) and 3-methoxyphenylboronic acid (0.409 g, 2.69 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.58 (s, 2H), 7.29 (t, J 7.8, 1H), 7.18-7.10 (m, 2H), 6.85 (dd, J 2, 8.1, 1H), 5.63 (s, 2H), 3.81 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08686048B2
Source datasetuspto-grants-2014_04
ORD IDord-d4ae9f3026bf411c9b0bdebf17265126
Source noteuspto-grants-2014_04