HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-dichloroaniline → HCID 66996749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-dichloroaniline | HCID 69680 | — |
| Reactant | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| Product | HCID 66996749 | HCID 66996749 | 102.6% |
Reaction Steps
The title compound (0.550 g) was prepared from 2,6-dichloro-4-bromoaniline (0.5 g, 2.0 mmol) and 3-methoxyphenylboronic acid (0.409 g, 2.69 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.58 (s, 2H), 7.29 (t, J 7.8, 1H), 7.18-7.10 (m, 2H), 6.85 (dd, J 2, 8.1, 1H), 5.63 (s, 2H), 3.81 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-d4ae9f3026bf411c9b0bdebf17265126 |
| Source note | uspto-grants-2014_04 |