HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-(trifluoromethoxy)aniline → HCID 46314437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-(trifluoromethoxy)aniline | HCID 737382 | — |
| Reactant | 2-Fluorophenylboronic acid | HCID 2734354 | — |
| Product | HCID 46314437 | HCID 46314437 | 57.1% |
Reaction Steps
The title compound (0.294 g) was prepared from 2-trifluoromethoxy-4-bromo aniline (0.5 g, 1.9 mmol) and 2-fluorophenylboronic acid (0.345 g, 2.5 mmol) as a yellow liquid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.47 (td, J 1.2, 4.7, 1H), 7.33-7.20 (m, 5H), 6.89 (d, J 8.8, 1H), 5.62 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-cffc5190ab8249b68f218eaaef8a22fe |
| Source note | uspto-grants-2014_04 |