HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-dichloroaniline → HCID 66997500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-dichloroaniline | HCID 69680 | — |
| Reactant | 2-Fluorophenylboronic acid | HCID 2734354 | — |
| Product | HCID 66997500 | HCID 66997500 | 75.4% |
Reaction Steps
The title compound (0.367 g) was prepared from 4-Bromo-2,6-dichloro aniline (0.5 g, 1.9 mmol) and 2-fluorophenylboronic acid (0.363 g, 2.6 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.50 (t, J 6.3, 1H), 7.43 (s, 2H), 7.39-7.31 (m, 1H), 7.29-7.21 (m, 2H), 5.73 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-1c5cb56ed45840449f6793fbe520f20c |
| Source note | uspto-grants-2014_04 |