HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Fluoro-5-methoxyphenyl)boronic acid → HCID 66997519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Fluoro-5-methoxyphenyl)boronic acid | HCID 2763243 | — |
| Reactant | 4-Bromo-2-chloro-6-fluoroaniline | HCID 20434620 | — |
| Product | HCID 66997519 | HCID 66997519 | 59.8% |
Reaction Steps
The title compound (71 mg) was prepared from 4-bromo-2-chloro-6-fluoroaniline (100 mg, 0.44 mmol) and 3-fluoro-5-methoxyphenylboronic acid (97 mg, 0.57 mmol) as a pale-yellow solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.51-7.45 (m, 2H), 7.05 (d, J 10.3, 1H), 7.00 (s, 1H), 6.73 (dd, J 2.1, 4.2, 1H), 5.60 (s, 2H), 3.81 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-221d167cfe8e452f88e53d062b22a276 |
| Source note | uspto-grants-2014_04 |