HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-chloro-6-fluoroaniline → HCID 66996801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-chloro-6-fluoroaniline | HCID 20434620 | — |
| Reactant | [3-(2,2,2-Trifluoroethoxy)phenyl]boronic acid | HCID 43145319 | — |
| Product | HCID 66996801 | HCID 66996801 | 60.4% |
Reaction Steps
The title compound (85 mg) was prepared from 4-bromo-2-chloro-6-fluoroaniline (100 mg, 0.44 mmol) and 3-(2,2,2-trifluoroethoxy)phenylboronic acid (127 mg, 0.57 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.53-7.44 (m, 2H), 7.38-7.26 (m, 3H), 6.94 (d, J 7, 1H), 5.55 (s, 2H), 4.83 (q, J 8.9, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-66f3b2adc0b2486ba27df7dbe05d1eeb |
| Source note | uspto-grants-2014_04 |