HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-3,5-difluoroaniline → 3'-(Ethylthio)-2,6-difluorobiphenyl-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-3,5-difluoroaniline | HCID 2736260 | — |
| Reactant | [3-(Ethylthio)phenyl]boronic acid | HCID 3484915 | — |
| Product | 3'-(Ethylthio)-2,6-difluorobiphenyl-4-amine | HCID 66997811 | 108.3% |
Reaction Steps
The title compound (500 mg) was prepared from 4-bromo-3,5-difluoroaniline (300 mg, 1.74 mmol) and 3-(ethylthio)phenylboronic acid (340 mg, 1.86 mmol) as a yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-db616d7db7dd4119932f86bfdc8eef93 |
| Source note | uspto-grants-2014_04 |