4-Bromoaniline → HCID 22256167, compound

HRID 2360465Notes

Reaction equation

Br[C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.[CH2:9]([C:11]1[CH:12]=[C:13](B(O)O)[CH:14]=[CH:15][CH:16]=1)[CH3:10]>>[CH2:9]([C:11]1[CH:16]=[C:15]([C:2]2[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=2)[CH:14]=[CH:13][CH:12]=1)[CH3:10]

Participants

Reactant 2

HCID 78074-Bromoaniline

HCID 16427138(3-Ethylphenyl)boronic acid

Product 1

HCID 22256167HCID 22256167, compoundYield 97.5%

Procedure

The title compound (300 mg) was prepared from 4-bromoaniline (270 mg, 1.56 mmol) and 3-ethylphenylboronic acid (300 mg, 2.04 mmol) as a colourless liquid.

Sources & evidence

ORD record: ord-c59b6452aa774dd98484bc7b64551d53
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08686048B2

Reaction notes

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