HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octylamine → HCID 53754231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | Dimethyl terephthalate | HCID 8441 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 70438889 | HCID 70438889 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53754231 | HCID 53754231 | 91% |
Reaction Steps
19.4 g (0.1 mole) of dimethyl terephthalate and 12.9 g (0.1 mole) of octylamine are refluxed for 8 hours in 100 ml of methanol together with 9 g (0.05 mole) of sodium methylate (30% strength). Working up as in Example 1 produces 26.5 g (91%) of 4-carbomethoxybenzoic acid octylamide having a 30% terephthalic acid bisoctylamide content.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642375 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-f49b4524fd334074983a54c5583434be |
| Source note | uspto-grants-1987_02 |