HCID 86654143, compound → HCID 178519361, compound

Participants

Reaction Steps

The title compound is prepared from 1H-benzoimidazole-5-carboxylic acid and a mixture of cis-8-benzyl-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline and cis-8-cyclohexylmethyl-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline (ca. 30:70) following a procedure analogous to that described in Example 1 and separated from the also formed Example 83 by HPLC on reversed phase (MeOH/H2O/NH4OH). Yield: 12% of theory; LC (method 1): tR=3.35 min; Mass spectrum (ESI+): m/z=422 [M+H]+.

Provenance & Evidence