HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178513601, compound → HCID 178509544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178513601 | HCID 178513601 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 178509544 | HCID 178509544 | 66% |
Reaction Steps
The title compound is prepared from cis-4-(1H-benzoimidazole-5-carbonyl)-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline-10-carboxylic acid amide following a procedure analogous to that described in Example 42. Yield: 66% of theory; TLC: rf=0.45 (silica gel, CH2Cl2/MeOH/32% aqueous NH3 90:10:1); Mass spectrum (ESI+): m/z=357 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686149B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-17c8a6d8bf8b454d912f1bb899999035 |
| Source note | uspto-grants-2014_04 |