HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroquinoline → 2-(1H-Indol-5-yl)quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroquinoline | HCID 11928 | — |
| Reactant | 1-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole | HCID 16217778 | — |
| Product | 2-(1H-Indol-5-yl)quinoline | HCID 58362351 | — |
Reaction Steps
2-(1H-indol-5-yl)quinoline was prepared using general procedure A from 2-chloroquinoline (32 mg, 0.2 mmol) and 1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole (51 mg, 0.2 mmol). The product was obtained as off-white solid (22 mg, 42%). MS (ESI): 245 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691187B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-2a972c5ad39d48b1a407766f2942987f |
| Source note | uspto-grants-2014_04 |