HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68484913, compound → HCID 68478391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68484913 | HCID 68484913 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 68478391 | HCID 68478391 | 83% |
Reaction Steps
To a solution of (2,4-dimethyl-1-vinylcyclohex-3-enyl)ethanol (20 mmol) in CH2Cl2 (40 ml) at room temperature was added PCC (40 mmol). The mixture was stirred at room temperature over night and was then diluted with hexane, filtered through a pad of celite and concentrated in vacuo. The residue was purified by chromatography to give 1-(2,4-dimethyl-1-vinylcyclohex-3-enyl)ethanone (83% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691746B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-793bae9246754f578c2bcc85e07fdbe6 |
| Source note | uspto-grants-2014_04 |