HRID2361860

反应详情

EQUATION

反应方程式

HRID 2361860 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 3-amino-5,6-bis(4-methylphenyl)-1,2,4-triazine (500 mg), methyl methanesulphonate (0.5 cm3) and methanol (10 cm3) was stirred at 40° for 24 hours and then evaporated to dryness. The resulting yellow solid was recrystallised from acetone giving the title compound as pale yellow needles,

WORKUP

后处理

  1. customevaporated to dryness
  2. customThe resulting yellow solid was recrystallised from acetone giving the title compound as pale yellow needles