HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diethoxyethylamine → HCID 42609175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | 8-Quinolinecarboxaldehyde | HCID 170103 | — |
| Product | HCID 42609175 | HCID 42609175 | 91.1% |
Reaction Steps
According to the procedure described in the synthesis method of Compound IX-2 with the modification that the reaction was carried out overnight, 2,2-diethoxyethanamine (2.18 ml, 15 mmol) was reacted with 8-quinolinecarboxaldehyde (1.89 g, 12 mmol) to obtain the title compound (3.0 g, 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691819B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-15cc0a6150704d1f96a43aee715e6cf0 |
| Source note | uspto-grants-2014_04 |