HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 66719111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | tert-Butyl {1-[4-(phenylacetyl)phenyl]cyclobutyl}carbamate | HCID 57805516 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 66719111 | HCID 66719111 | — |
Reaction Steps
To a solution of compound 1-3 (5.0 g, 13.7 mmol) in toluene (30 mL) was added DMFDMA (18.15 g, 68.4 mmol) and the mixture was heated at reflux for 4 hours. The TLC showed the starting material was disappeared. The mixture was cooled and the formed white solid was collected. After washed by PE, the solid was dried in vacuum to get the product 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691825B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-8c6d2d1f2ffe48f480172971da07ad95 |
| Source note | uspto-grants-2014_04 |