HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86678225, compound → HCID 71509868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86678225 | HCID 86678225 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Trimethylamine | HCID 1146 | — |
| Product | HCID 71509868 | HCID 71509868 | 111.1% |
Reaction Steps
Intermediate 15 (105 mg, 0.16 mmol) was dissolved in a solution of 31% trimethylamine in ethanol. The reaction mixture was stirred at RT for 16 hours and then filtered. The solid was collected by filtration and dried in vacuo to yield the title compound as a white solid (62 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691826B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-c15bda9fc1c84edca65ce108a6d380d0 |
| Source note | uspto-grants-2014_04 |